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          Document History for Document ID 28500

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Document Version Version Comment Date Status
28500.0 [No comment] 04.07.2006 14:21 Released

ID: 28500.0, MPI für Polymerforschung / MPI Polymerforschung
Dipolar recoupling in NOESY-Type H-1-H-1 NMR experiments under HRMAS conditions
Authors:Thieme, K.; Zech, G.; Kunz, H.; Spiess, Hans Wolfgang; Schnell, Ingo
Language:English
Date of Publication (YYYY-MM-DD):2002-05-02
Title of Journal:Organic Letters
Journal Abbrev.:Org. Lett.
Volume:4
Issue / Number:9
Start Page:1559
End Page:1562
Review Status:No review
Audience:Not Specified
Abstract / Description:The concept of dipolar recoupling is introduced to H-1-H-1 NOESY experiments performed under HRMAS conditions. Dipole- dipole couplings are selectively recoupled during the mixing period, while MAS ensures high resolution in the spectral dimensions. Incoherent dipolar exchange is replaced by amplified coherent processes, such that time scales for polarization transfer are shortened, and dipolar double-quantum techniques become applicable. In this way, dipole-dipole couplings, as well as J-couplings, can be individually measured.
Comment of the Author/Creator:Date: 2002, MAY 2
External Publication Status:published
Document Type:Article
Affiliations:MPI für Polymerforschung
External Affiliations:Univ Mainz, Inst Organ Chem, D-55099 Mainz, Germany
Identifiers:ISI:000175243900038 [ID No:1]
ISSN:1523-7060 [ID No:2]
LOCALID:P-02-25